Table T9. Estimates of accuracy and precision for JY2000 ICP-AES major element analyses.
Sample run or replicate | Date (Dec 1999) |
Major element (wt%) | Total | |||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|
SiO2 | TiO2 | Al2O3 | Fe2O3 | MnO | MgO | CaO | Na2O | K2O | P2O5 | |||
MW8801-17-26 (whole rock)* | ||||||||||||
Probe | 50.62 | 1.36 | 15.49 | 9.29 | 0.15 | 8.37 | 11.54 | 2.93 | 0.03 | 0.15 | 99.93 | |
DCP | 50.17 | 1.29 | 15.61 | 9.49 | 0.16 | 8.61 | 11.73 | 2.83 | 0.03 | 0.12 | 100.04 | |
Leg187A | 1 | 51.27† | 1.32 | 15.21 | 9.38 | 0.16 | 8.56 | 11.40 | 2.54 | 0.04 | 0.13 | 100† |
Leg187C | 3 | 50.69 | 1.32 | 15.21 | 9.38 | 0.16 | 8.56 | 11.40 | 2.54 | 0.04 | 0.13 | 99.41 |
Leg187D.a | 8 | 50.56 | 1.24 | 14.80 | 9.46 | 0.16 | 8.45 | 11.52 | 2.54 | 0.03 | 0.12 | 98.88 |
Leg187D.b | 8 | 50.73 | 1.23 | 15.16 | 9.34 | 0.16 | 8.20 | 11.89 | 2.68 | 0.05 | 0.13 | 99.58 |
Leg187E.a | 13 | 50.84 | 1.35 | 15.38 | 9.63 | 0.16 | 8.59 | 11.62 | 2.83 | 0.04 | 0.13 | 100.56 |
Leg187E.b | 13 | 50.65 | 1.33 | 15.59 | 9.51 | 0.16 | 8.46 | 11.77 | 2.74 | 0.04 | 0.13 | 100.36 |
Leg187E.c | 13 | 51.23 | 1.33 | 15.76 | 9.54 | 0.16 | 8.46 | 11.74 | 2.77 | 0.04 | 0.13 | 101.16 |
Leg187E.d | 13 | 51.07 | 1.35 | 15.75 | 9.74 | 0.16 | 8.61 | 11.92 | 2.91 | 0.03 | 0.13 | 101.67 |
Leg187F.a | 14 | 49.91 | 1.31 | 15.25 | 9.49 | 0.16 | 8.54 | 11.54 | 2.67 | 0.04 | 0.13 | 99.04 |
Leg187F.b | 14 | 49.48 | 1.29 | 15.42 | 9.32 | 0.16 | 8.45 | 11.60 | 2.65 | 0.04 | 0.12 | 98.53 |
Leg187G.a | 17 | 50.86 | 1.33 | 15.33 | 9.66 | 0.16 | 8.45 | 11.56 | 2.76 | 0.05 | 0.12 | 100.29 |
Leg187G.b | 17 | 50.85 | 1.32 | 15.35 | 9.67 | 0.17 | 8.67 | 11.64 | 3.06 | 0.04 | 0.13 | 100.89 |
Leg187H.a | 20 | 49.94 | 1.31 | 15.57 | 9.48 | 0.16 | 8.31 | 11.60 | 2.91 | 0.05 | 0.12 | 99.44 |
Leg187H.b | 20 | 51.32 | 1.36 | 15.64 | 9.75 | 0.16 | 8.58 | 11.90 | 2.95 | 0.05 | 0.12 | 101.83 |
Leg187H.c | 20 | 50.53 | 1.29 | 15.40 | 9.64 | 0.16 | 8.55 | 11.61 | 2.95 | 0.05 | 0.13 | 100.31 |
Leg187I.a | 26 | 50.22 | 1.34 | 15.47 | 9.44 | 0.15 | 8.42 | 11.63 | 2.87 | 0.06 | 0.11 | 99.72 |
Leg187I.b | 26 | 50.24 | 1.28 | 15.24 | 9.26 | 0.17 | 8.26 | 11.56 | 3.14 | 0.06 | 0.15 | 99.36 |
Average: | 50.61 | 1.31 | 15.38 | 9.51 | 0.16 | 8.48 | 11.64 | 2.79 | 0.05 | 0.13 | ||
1 SD: | 0.52 | 0.04 | 0.24 | 0.150 | 0.00 | 0.13 | 0.16 | 0.181 | 0.009 | 0.007 | ||
%RSD: | 1.02 | 2.73 | 1.57 | 1.58 | 2.67 | 1.49 | 1.34 | 6.49 | 19.62 | 5.79 | ||
BHVO-2 | ||||||||||||
Published value | 49.9 | 2.73 | 13.5 | 12.3 | 0.166 | 7.23 | 11.4 | 2.22 | 0.52 | 0.27 | 100.236 | |
± | 0.6 | 0.04 | 0.2 | 0.2 | 0.12 | 0.2 | 0.08 | 0.01 | 0.02 | |||
Leg187C | 3 | 48.28† | 2.77 | 14.71 | 12.33 | 0.17 | 7.46 | 10.99 | 2.40 | 0.58 | 0.31 | 100† |
Leg187D | 8 | 50.08 | 2.57 | 12.91 | 11.98 | 0.17 | 7.11 | 11.27 | 2.19 | 0.49 | 0.28 | 99.04 |
Leg187E.a | 13 | 49.50 | 2.72 | 14.12 | 12.10 | 0.17 | 7.25 | 11.50 | 2.12 | 0.44 | 0.28 | 100.20 |
Leg187E.b | 13 | 48.92 | 2.69 | 14.22 | 12.18 | 0.16 | 7.14 | 11.41 | 2.02 | 0.44 | 0.28 | 99.48 |
Leg187E.c | 13 | 49.86 | 2.79 | 14.34 | 12.32 | 0.17 | 7.18 | 11.52 | 2.27 | 0.41 | 0.28 | 101.15 |
Leg187E.d | 13 | 49.40 | 2.75 | 14.14 | 12.51 | 0.17 | 7.25 | 11.52 | 2.17 | 0.44 | 0.27 | 100.62 |
Leg187F.a | 14 | 48.97 | 2.66 | 13.72 | 12.07 | 0.17 | 7.25 | 11.26 | 2.06 | 0.41 | 0.27 | 98.83 |
Leg187F.b | 14 | 50.05 | 2.73 | 13.82 | 12.31 | 0.17 | 7.13 | 11.46 | 2.06 | 0.40 | 0.24 | 100.37 |
Leg187G.a | 17 | 48.93 | 2.70 | 13.42 | 12.32 | 0.17 | 7.20 | 11.23 | 2.14 | 0.52 | 0.27 | 98.90 |
Leg187G.b | 17 | 48.63 | 2.66 | 13.41 | 12.10 | 0.17 | 7.20 | 11.12 | 2.45 | 0.53 | 0.31 | 98.59 |
Leg187H.a | 20 | 48.83 | 2.66 | 13.81 | 11.98 | 0.16 | 7.04 | 11.27 | 2.19 | 0.54 | 0.25 | 98.74 |
Leg187H.b | 20 | 49.62 | 2.73 | 13.86 | 12.04 | 0.17 | 7.36 | 11.53 | 2.27 | 0.54 | 0.28 | 100.39 |
Leg187H.c | 20 | 48.21 | 2.61 | 13.40 | 11.81 | 0.16 | 7.08 | 11.08 | 2.00 | 0.57 | 0.29 | 97.19 |
Leg187I.a | 26 | 49.06 | 2.66 | 13.66 | 12.10 | 0.17 | 7.19 | 11.21 | 2.24 | 0.52 | 0.26 | 99.08 |
Average: | 49.17 | 2.69 | 13.82 | 12.15 | 0.17 | 7.20 | 11.31 | 2.18 | 0.49 | 0.28 | ||
1 SD: | 0.61 | 0.06 | 0.46 | 0.185 | 0.00 | 0.11 | 0.18 | 0.13 | 0.06 | 0.018 | ||
%RSD: | 1.23 | 2.30 | 3.35 | 1.52 | 1.76 | 1.52 | 1.59 | 6.14 | 13.12 | 6.40 |
Notes: These estimates are derived from replicate analyses of the USGS reference standard BHVO-2 and Zone A SEIR whole-rock basalt sample MW8801-17-26, Leg 187. * = D. Pyle and D. Christie (unpubl. data), microprobe and direct current plasma (DCP) analyses. † = SiO2 estimated by subtracting the total of the other major elements from 100%. SD = standard deviation, RSD = relative standard deviation. This table is also available in ASCII format.