Parameter
|
Method
|
SCO-1 value
|
Analytical uncertainty
|
||
---|---|---|---|---|---|
Accepted
|
Measured
|
1 (%)
|
n
|
||
Nitrogen | Gas chromatography |
|
|
5.8 | 6 |
Carbon | Gas chromatography |
|
|
1.5 | 6 |
Hydrogen | Gas chromatography |
|
|
5.3 | 6 |
Sulfur | Gas chromatography |
|
|
BDL |
|
%CaCO3 | Coulometry |
|
|
1.1 | 5 |
SiO2 | ICP-AES | 62.78 ± 0.66 | 64.68 | 3.4 | 6 |
Al2O3 | ICP-AES | 13.67 ± 0.21 | 13.58 | 5.0 | 6 |
TiO2 | ICP-AES | 0.63 ± 0.06 | 0.61 | 5.8 | 6 |
Fe2O3T | ICP-AES | 5.13 ± 0.18 | 5.03 | 7.1 | 6 |
MnO | ICP-AES | 0.05 ± 0.003 | 0.05 | 2.9 | 6 |
CaO | ICP-AES | 2.62 ± 0.20 | 2.52 | 1.5 | 6 |
MgO | ICP-AES | 2.72 ± 0.18 | 2.73 | 3.9 | 6 |
Na2O | ICP-AES | 0.90 ± 0.06 | 0.92 | >20 | 6 |
K2O | ICP-AES | 2.77 ± 0.08 | 2.76 | >20 | 6 |
Sr | ICP-AES | 170 ± 16 | 168 | 2.7 | 6 |
Ba | ICP-AES | 570 ± 30 | 578 | 6.9 | 6 |
Cr | ICP-AES | 68 ± 5 | 65 | >20 | 6 |
Ni | ICP-AES | 27 ± 4 | 25 | 13.1 | 6 |
V | ICP-AES | 131 | 129 | 10.2 | 6 |
Y | ICP-AES | 26 ± 4 | 29 | 8.5 | 6 |
Note: Major element oxides are reported as weight percent and trace elements as parts per million. SCO-1 = Cody Shale, a silty shale sediment standard. BDL = below detection limit. ICP-AES = inductively coupled plasma-atomic emission spectroscopy. n = number of analyses. This table is also available in ASCII.