Table T11. Sediment chemistry analyses and corresponding reproducibility.
Parameter
Method
SCO-1 value
Analytical uncertainty
Accepted
Measured
1 (%)
n
Nitrogen Gas chromatography

5.8 6
Carbon Gas chromatography

1.5 6
Hydrogen Gas chromatography

5.3 6
Sulfur Gas chromatography

BDL
%CaCO3 Coulometry

1.1 5
SiO2 ICP-AES 62.78 ± 0.66 64.68 3.4 6
Al2O3 ICP-AES 13.67 ± 0.21 13.58 5.0 6
TiO2 ICP-AES 0.63 ± 0.06 0.61 5.8 6
Fe2O3T ICP-AES 5.13 ± 0.18 5.03 7.1 6
MnO ICP-AES 0.05 ± 0.003 0.05 2.9 6
CaO ICP-AES 2.62 ± 0.20 2.52 1.5 6
MgO ICP-AES 2.72 ± 0.18 2.73 3.9 6
Na2O ICP-AES 0.90 ± 0.06 0.92 >20 6
K2O ICP-AES 2.77 ± 0.08 2.76 >20 6
Sr ICP-AES 170 ± 16 168 2.7 6
Ba ICP-AES 570 ± 30 578 6.9 6
Cr ICP-AES 68 ± 5 65 >20 6
Ni ICP-AES 27 ± 4 25 13.1 6
V ICP-AES 131 129 10.2 6
Y ICP-AES 26 ± 4 29 8.5 6

Note: Major element oxides are reported as weight percent and trace elements as parts per million. SCO-1 = Cody Shale, a silty shale sediment standard. BDL = below detection limit. ICP-AES = inductively coupled plasma-atomic emission spectroscopy. n = number of analyses. This table is also available in ASCII.