APPENDIX Q

X-Ray Diffraction Analyses

Janus XRD data model. (See PDF version.)

Description of data items from XRD query. (See PDF version.)

XRD Data Header Format

Legs 147–164
SampleIdent,894A 1R2 130-135 GLY,/
 DiffrType,PW1710,/
 DiffrNumber,1,/
 Anode,Cu,/
 DivergenceSlit,Automatic, 12,/
 MonochromatorUsed,YES,/
 GeneratorVoltage, 40,/
 TubeCurrent, 35,/
 FileDateTime, 8-dec-1992 23:58,/
 DataAngleRange, 2.0000, 23.9900,/
 ScanStepSize, 0.010,/
 ScanType,CONTINUOUS,/
 ScanStepTime, 1.00,/
 RawScan
 272, 240, 225, 269, 234, 243, 196, 213
 243, 231, 199, 202, 204, 188, 193, 222
 166, 185, 199, 182, 159, 169, 182, 166
 . . .
 169, 159, 193, 166, 164, 182, 177, 185
 /
Legs 165–180
SampleIdent,49A10X314,/
 Title1,Ocean Drilling Program,/
 Title2,PC-APD Software Version 3.6f,/
 DiffrType,PW1710,/
 DiffrNumber,1,/
 Anode,Cu,/
 LabdaAlpha1, 1.54056,/
 LabdaAlpha2, 1.54439,/
 RatioAlpha21, 0.50000,/
 DivergenceSlit,Automatic, 12,/
 ReceivingSlit,0.2,/
 MonochromatorUsed,YES,/
 GeneratorVoltage, 40,/
 TubeCurrent, 35,/
 FileDateTime,22-Jan-1997 1:39,/
 DataAngleRange, 2.0000, 60.0000,/
 ScanStepSize, 0.020,/
 ScanType,STEP,/
 ScanStepTime, 1.00,/
 RawScan
 17, 15, 9, 9, 18, 11, 13, 19
 15, 13, 20, 11, 18, 15, 17, 8
 19, 9, 17, 23, 18, 15, 11, 24
 . . .
 32, 19, 35, 35, 26,/
Legs 181–210
SampleIdent,ss001552434 bulk,/
 Title1,,/
 Title2,PC-APD Software Version 3.6f,/
 DiffrType,PW1710,/
 DiffrNumber,1,/
 Anode,Cu,/
 LabdaAlpha1,1.54056,/
 LabdaAlpha2,1.54439,/
 RatioAlpha21,.5,/
 DivergenceSlit,Automatic,12,/
 ReceivingSlit,.2,/
 MonochromatorUsed,YES,/
 GeneratorVoltage,40,/
 TubeCurrent,35,/
 FileDateTime,10-Aug-2003 06:56,/
 DataAngleRange,2,70,/
 ScanStepSize,.02,/
 ScanType,STEP,/
 ScanStepTime,1,/
 Rawscan,/
 365, 342, 361, 369, 313, 361, 310, 310
 339, 313, 303, 328, 328, 350, 299, 286
 289, 256, 276, 289, 279, 313, 266, 282
 . . .
 193,/

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