5. Data Report: Normalization Factors for Semiquantitative X-Ray Diffraction Analysis, with Application to DSDP Site 297, Shikoku Basin1

Michael B. Underwood,2 Nandini Basu,2 Joan Steurer,2 and Swati Udas2

ABSTRACT

This data report documents the acquisition of two new sets of normalization factors for semiquantitative X-ray diffraction analyses. One set of factors is for bulk sediment powders, and the other applies to oriented aggregates of clay-sized fractions (<2 µm). We analyzed mixtures of standard minerals with known weight percentages of each component and solved for the normalization factors using matrix singular value decomposition. The components in bulk powders include total clay minerals (a mixture of smectite, illite, and chlorite), quartz, plagioclase, and calcite. For clay-sized fractions, the minerals are smectite, illite, chlorite, and quartz. We tested the utility of the method by analyzing natural mudstone specimens from Site 297 of the Deep Sea Drilling Project, which is located in the Shikoku Basin south of Site 1177 of the Ocean Drilling Program (Ashizuri transect).

1Underwood, M., Basu, N., Steurer, J., and Udas, S., 2003. Data report: Normalization factors for semiquantitative X-ray diffraction analysis, with application to DSDP Site 297, Shikoku Basin. In Mikada, H., Moore, G.F., Taira, A., Becker, K., Moore, J.C., and Klaus, A. (Eds.), Proc. ODP, Sci. Results, 190/196 [Online]. Available from World Wide Web: <http://www-odp.tamu.edu/publications/190196SR/203/203.htm>. [Cited YYYY-MM-DD]

2Department of Geological Sciences, University of Missouri, Columbia MO 65211, USA. Correspondence author: UnderwoodM@missouri.edu

Initial receipt: 4 November 2002
Acceptance: 6 June 2003
Web publication: 22 August 2003
Ms 190SR-203

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